Synthesis and characterization of cis and trans‐4‐d−1‐1‐tetralol

G. S. Groenewold; M. L. Gross

doi:10.1002/jlcr.2580181214

Synthesis and characterization of cis and trans‐4‐d₋₁‐1‐tetralol

G. S. Groenewold, M. L. Gross

Research output: Contribution to journal › Article › peer-review

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Abstract

Trans‐4‐d₋₁‐tetranydronaphthalen‐1‐ol (trans‐4‐d₋₁‐1‐ tetralol) was synthesized from 1,4‐epoxy‐1,2,3,4‐ tetrahydronaphthalene using lithium tri‐tert‐butoxyaluminodeuteride. Cis‐4‐d₋₁‐1‐tetralol was made by epimerizing the trans‐ compound. Both compounds were characterized by high field 360 MHz NMR spectroscopy.

Original language	English
Pages (from-to)	1809-1816
Number of pages	8
Journal	Journal of Labelled Compounds and Radiopharmaceuticals
Volume	18
Issue number	12
DOIs	https://doi.org/10.1002/jlcr.2580181214
State	Published - Dec 1981

Keywords

NMR
epimerization
lithium tri‐tert‐butoxyaluminodeuteride
mass spectrometry
tetralol

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title = "Synthesis and characterization of cis and trans‐4‐d−1‐1‐tetralol",

abstract = "Trans‐4‐d−1‐tetranydronaphthalen‐1‐ol (trans‐4‐d−1‐1‐ tetralol) was synthesized from 1,4‐epoxy‐1,2,3,4‐ tetrahydronaphthalene using lithium tri‐tert‐butoxyaluminodeuteride. Cis‐4‐d−1‐1‐tetralol was made by epimerizing the trans‐ compound. Both compounds were characterized by high field 360 MHz NMR spectroscopy.",

keywords = "NMR, epimerization, lithium tri‐tert‐butoxyaluminodeuteride, mass spectrometry, tetralol",

author = "Groenewold, {G. S.} and Gross, {M. L.}",

year = "1981",

month = dec,

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pages = "1809--1816",

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T1 - Synthesis and characterization of cis and trans‐4‐d−1‐1‐tetralol

AU - Groenewold, G. S.

AU - Gross, M. L.

PY - 1981/12

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N2 - Trans‐4‐d−1‐tetranydronaphthalen‐1‐ol (trans‐4‐d−1‐1‐ tetralol) was synthesized from 1,4‐epoxy‐1,2,3,4‐ tetrahydronaphthalene using lithium tri‐tert‐butoxyaluminodeuteride. Cis‐4‐d−1‐1‐tetralol was made by epimerizing the trans‐ compound. Both compounds were characterized by high field 360 MHz NMR spectroscopy.

AB - Trans‐4‐d−1‐tetranydronaphthalen‐1‐ol (trans‐4‐d−1‐1‐ tetralol) was synthesized from 1,4‐epoxy‐1,2,3,4‐ tetrahydronaphthalene using lithium tri‐tert‐butoxyaluminodeuteride. Cis‐4‐d−1‐1‐tetralol was made by epimerizing the trans‐ compound. Both compounds were characterized by high field 360 MHz NMR spectroscopy.

KW - NMR

KW - epimerization

KW - lithium tri‐tert‐butoxyaluminodeuteride

KW - mass spectrometry

KW - tetralol

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DO - 10.1002/jlcr.2580181214

M3 - Article

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SN - 0362-4803

VL - 18

SP - 1809

EP - 1816

JO - Journal of Labelled Compounds and Radiopharmaceuticals

JF - Journal of Labelled Compounds and Radiopharmaceuticals

IS - 12

ER -

Synthesis and characterization of cis and trans‐4‐d₋₁‐1‐tetralol

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Keywords

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