TY - JOUR
T1 - Naphthaceno[5,6-cd]-1,2-dithiole, C18H10S2
AU - Katz, Henry
AU - Conturo, Thomas E.
AU - Nigrey, Paul J.
AU - Donohue, Jerry
PY - 1983/6
Y1 - 1983/6
N2 - C18H10S2, M=290.34, monoclinic, P21, a=20.556(5), b=15.843(3), c=3.963(1) Å, β=92.79(2)° at 18°C, Z=4, Dx=1.496 g cm-3, μ(Cu Kα)=3.53 mm-1. Full-matrix least-squares refinement resulted in a final conventional R value of 0.036 for 2030 observed reflections. The average C-S bond distance is 1.747(16) Å, the S-S bond length is 2.074(1) Å. The torsion angles at the disulfide group are close to zero, at 3.5 and 0.8°. The carbon frameworks are nearly planar, and closely approximate symmetry mmm. Bond distances are comparable with those in related molecules.
AB - C18H10S2, M=290.34, monoclinic, P21, a=20.556(5), b=15.843(3), c=3.963(1) Å, β=92.79(2)° at 18°C, Z=4, Dx=1.496 g cm-3, μ(Cu Kα)=3.53 mm-1. Full-matrix least-squares refinement resulted in a final conventional R value of 0.036 for 2030 observed reflections. The average C-S bond distance is 1.747(16) Å, the S-S bond length is 2.074(1) Å. The torsion angles at the disulfide group are close to zero, at 3.5 and 0.8°. The carbon frameworks are nearly planar, and closely approximate symmetry mmm. Bond distances are comparable with those in related molecules.
UR - http://www.scopus.com/inward/record.url?scp=34250144821&partnerID=8YFLogxK
U2 - 10.1007/BF01161516
DO - 10.1007/BF01161516
M3 - Article
AN - SCOPUS:34250144821
VL - 13
SP - 221
EP - 229
JO - Journal of Crystallographic and Spectroscopic Research
JF - Journal of Crystallographic and Spectroscopic Research
SN - 0277-8068
IS - 3
ER -